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Beilstein J. Org. Chem. 2018, 14, 2974–2990, doi:10.3762/bjoc.14.277
Graphical Abstract
Figure 1: Structures of fungal volatiles. Trichodiene (1), aristolochene (2), (R)-oct-1-en-3-ol (3), 3,4-dime...
Figure 2: Total ion chromatogram of a CLSA headspace extract from Hypoxylon griseobrunneum MUCL 53754. Peak n...
Figure 3: Volatiles from Hypoxylon griseobrunneum.
Figure 4: EI mass spectra of A) 2,4,5-trimethylanisole (24), B) the coeluting mixture of 3,4-dimethylanisole (...
Scheme 1: Synthesis of trimethylanisoles 24 and 24d.
Scheme 2: Hypothetical biosynthesis of 24. ACP: acyl carrier protein, AT: acyl transferase, KR: ketoreductase...
Figure 5: Biosynthesis of 24. Feeding of (methyl-2H3)methionine resulted in the incorporation of labelling in...
Scheme 3: Hypothetical biosynthesis of 25 and 26.
Figure 6: Total ion chromatogram of a CLSA headspace extract from Hypoxylon macrocarpum STMA 130423. Peak num...
Figure 7: Volatiles from Hypoxylon macrocarpum.
Figure 8: EI mass spectra of A) 3,4-dimethoxybenzaldehyde (42), B) 3,4,5-trimethoxytoluene (44), and C) 2,4,5...
Scheme 4: Synthesis of 2,3,4-trimethoxytoluene (44a).